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The
NATLSCO Air Sampling Guide is meant as a quick reference
for media and flow rates. Analytes can be searched either
by chemical name
or Chemical Abstract
System Number (CASN). Symbols or
numbers indicating isomers or structures are given after
the chemical name; e.g., N-methyl-2-Pyrrolidone is listed
as methyl-2-Pyrrolidone (N). An asterisk is used as
a wild card for the chemical name. The CAS# must be
input as an exact match, including appropriate hyphenation
(-).
If you do not find a particular compound by either chemical
name or CASN, please email
us with your request and we will do a search to see
if an appropriate method exists.
Please remember, the Air Sampling Guide is meant as
a reference to follow when sampling for chemical contaminants
that may be found in a workplace environment. The guidelines
closely parallel the recommendations of OSHA
or NIOSH. If the Air Sampling Guide is used for other
types of sampling such as Indoor Air Quality, Ambient
Air Monitoring or Short Term Sampling, the flow rates
and maximum air volumes may have to be modified. Please
call the laboratory to discuss your specific sampling
criteria.
ANALYTE SEARCH:
For example, if you wish to search for Benzene, type
either Benzene
or Benz* in
the Analyte section. A list of 17 different Analytes
-- ranging from Benzene, Benzene (STEL), Ethyl Benzene,
Benzene Solubles or the Trimethyl Benzene isomers --
will be returned to you. Simply click on the compound
of interest and you will have a screen showing you the
summary of the sampling method. This summary includes:
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Media
-
Method
-
Flow Rate
-
CAS#
-
Minimum Volume
-
Maximum Volume
CAS Number SEARCH:
Enter the appropriate CAS number, for example
111-76-2 in the CAS Number field
and hit the search button. Four chemical names are displayed:
-
Butoxyethanol (2)
-
Butyl Cellosolve
-
Ethylene Glycol Monobutyl Ether
-
CAS#
-
Polysolve EB
These are all chemical synonyms for the same chemical
compound. Again, simply click on the compound of interest
and you will have a screen show the summary of the sampling
method.
Flow
Rates and Volumes are meant as guidelines.
Short-term sampling can normally be done at faster flow
rates. However, this depends on several factors including
concentration, length of time, volatility of Analyte
and media.
Analytes taken on media that requires derivitization
such as isocyanate sampling; formaldehyde, etc. have
been validated for very specific sampling rates. There
must be sufficient contact time between the analyte
and the derivative to form the complex.
Where possible, NATLSCO uses large bed solid sorbent
tubes to allow for maximum flexibility. All charcoal
tubes provided by the lab are 600-mg tubes (400-mg front
section and 200 mg back section). Solid sorbent tubes
are normally designed to have a 2:1 ratio in the front
to back section. This is designed to verify validity
of results. Samples containing more than 25% of the
analyte in the back section are considered by OSHA
to be invalid samples. Please note that most reference
to Charcoal Tubes in the media section have a media
code of CT2. This notation reflects the new type of
charcoal type material that is being supplied by all
major distributors. Many of the chemical compounds show
enhanced desorption efficiencies using the new media.
Some of the analytes may show two different types of
media such as CT2/OR90. This type of notation indicates
that we have evaluated the material on both types of
media. You may need to check with the laboratory for
compatibility of compounds.
*
-- Next to any media indicates that analyte should be
taken separately because of special digestion or extraction
requirements. Although some compounds, such as the Cellosolves,
are desorbed in similar solvents, it is best to check
with the laboratory for compatibility.
Other solid sorbents, such as OR90 or Silica gel, may
use the same tube, but again, require different desorbing
agents or analysis. An example of this would be a Silica
Gel tube, which can be used for either Methanol or Phenol.
The tube would be desorbed in water to analyze for methanol,
but desorbed in acetone for Phenol analysis.
**
-- A bulk of the material must be submitted under separate
cover. Samples are analyzed using the bulk material
as a standard.
The NATLSCO Laboratory will provide you with the
appropriate sampling media. Please call the Lab at (888)-576-7522,
email
us or use the Media
Order Form.
Please note that every effort has been made to assure
the accuracy of the Air Sampling Guide. Notify the NATLSCO
laboratory if you find any errors.
If
you would like more information, send an email to thomas.oberstar@us.bureauveritas.com
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